"Solid Phase Extraction"

Supplier: Merck

Monolinuron CRM may also be used as given below: Determination of 252 pesticides extracted from surface water samples by solid-phase extraction (SPE) using liquid chromatography quadrupole-orbitrap high-resolution tandem mass spectrometry. Extraction of 13 pesticides from four groundwater and three river water samples using silica-based MSU-1 mesoporous solid as a sorbent for their solid-phase extraction (SPE) followed by ultra-performance liquid chromatography-triple quadrupole-mass spectrometric (UHPLC- QqQ-MS/MS) determination. Development and validation of a UHPLC-diode array detection (DAD) method for simultaneous determination of urea and tebuthiuron herbicides in four fresh vegetable samples. Multi-residue analysis of 50 herbicides in 51 grain samples of soybean corn and wheat by ultra-performance liquid chromatography-electrospray ionisation-mass spectrometry (UPLC-ESI-MS). Extraction of 109 pesticide residues from different chemical classes from 345 tomato samples by modified QuEChERS method and their determination using liquid chromatography-tandem mass spectrometry (LC-MS/MS). Simultaneous analysis of 238 pesticides and 78 veterinary drugs in 80 bovine milk samples using ultra-fast liquid chromatography-tandem mass spectrometry (UFLC-MS/MS) and gas chromatography-tandem mass spectrometry (GC-MS/MS).

Supplier: VARIAN

Bond Elut™ PCB is a specially designed sorbent which allows for the facile extraction of polychlorinated biphenyl (PCB) compounds from a variety of matrices. Desired analytes can be loaded and eluted using a simple, single solvent method prior to analysis by GC/ECD.

Supplier: VARIAN

Florisil is a magnesia-loaded silica gel, extremely polar in nature and ideal for the isolation of polar compounds from non-polar matrices.

Supplier: GILSON LCMS

This ASPEC® system for positive pressure solid phase extraction (SPE) automation maximises throughput by processing up to four samples in parallel. With its small footprint and multiple probes, it is the ideal choice for reproducible and efficient sample cleanup for clinical, forensic, doping, food, and environmental testing labs.

Supplier: VARIAN

Bond Elut™ LMS polymeric sorbent lets you elute without having to add amine modifiers, buffers, or acids. The elimination of secondary interactions means that elution of analytes can be achieved with pure organic solvents or HPLC mobile phase-compatible solvent mixtures of low ionic strength. These characteristics are crucial to allow compatibility with LC/MS or other delicate analytical techniques.

Supplier: VARIAN

Bond Elut™ PH is a non-polar bonded silica material which exhibits a different selectivity to alkyl or aliphatic functionalised phases such as C8 or cyclohexyl. The electron density present in the aromatic ring affords an enhancement in the retention of conjugated or aromatic ring-containing analytes due to desirable pi-pi interactions.

Supplier: VARIAN

Due to the methyl group and subsequent low carbon load, Bond Elut™ C1 is the least retentive of all alkyl group bonded phases for non-polar compounds. However, due to the extensive end capping of this sorbent to mask polar silanol activity, retention and elution of polar and multi-functional analytes can still be achieved. Typical applications include plasma, urine and aqueous samples.

Supplier: VARIAN

Bond Elut™ PPL is a styrene-divinylvenzene (SDVB) polymer that has been modified with a proprietary non-polar surface. PPL will retain even the most polar classes of analytes, including phenols. The large particle size allows ease of flow for viscous or particulate rich water samples, while the high surface area and strong hydrophobicity ensure reproducible extractions with high recoveries upon elution. Bond Elut™ PPL is suitable for EPA Method 528 ‘Determination of Phenols in Drinking Water by SPE and Capillary GC/MS’.

Supplier: VARIAN

Bond Elut™ C18 OH is a non-end capped version of the octadecyl bonded phases that enables the silanols on the silica surface to be more active. This low-load C18 has well-controlled silanol activity that permits the fractionation of metabolites and enhances retention of basic compounds compared to an endcapped C18. The pore size makes it a good choice for peptide extraction.

Supplier: VARIAN

CBA is a mid-polarity sorbent and weak cation exchanger (pKa 4,8). It can be used with a wider range of counter-ions than lower pKa sorbents like SCX and will demonstrate easier elution of quaternary amine functionalised analytes.

Supplier: Merck

Tebutam CRM may also be used as given below:
Optimisation of sample extraction based on QuEChERS and dispersive-solid-phase extraction (d-SPE) clean-up for the multi-residue analysis of 120 pesticides 16 polycyclic aromatic hydrocarbons and 22 polychlorinated biphenyls by liquid and gas chromatography coupled with tandem mass spectrometry (MS/MS)
Evaluation of 250 pesticide residues extracted by QuEChERS method from 103 processed fruit samples using ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS)
Determination of 90 pesticides 16 polycyclic aromatic hydrocarbons and 22 polychlorinated biphenyls in honey samples by using QuEChERS combined with dispersive solid-phase extraction (SPME) for sample pre-treatment and liquid chromatography-triple-quadrupole tandem mass spectrometry and gas chromatography-ion-trap tandem mass spectrometry for quantitation
Screening and quantification of 569 pesticides in honeysuckle samples by a combination of ultrahigh-performance liquid chromatography (UHPLC) and quadrupole-Orbitrap high-resolution mass spectrometry
Simultaneous determination of 134 pesticide residues in tea samples using d-SPE extraction with a multi-functional filter (MFF) followed by ultra-high performance liquid chromatography (UPLC) and quadrupole time-of-flight mass spectrometry (TOF-MS).

Supplier: VARIAN

Bond Elut™ CH is a mid-polarity sorbent that exhibits unique selectivities for certain analytes. When employed as a non-polar sorbent, CH has the approximate polarity of a C₂ sorbent. Bond Elut™ CH is often a good choice when non-polar sorbents such as C₁₈, C₈ or C₂ do not provide the desired selectivity.

Supplier: VARIAN

Solid phase microextraction (SPME) is a technique for extracting analytes from solid, liquid or gaseous samples by adsorbing them onto the SPME fiber and then desorbing them into an inlet, either on a gas chromatograph (GC) or an HPLC system. SPME is amenable to automation using an autosampler or it can be performed manually as well.

Supplier: VARIAN

Bond Elut™ Certify II was developed specifically for the rapid and effective extraction of acidic drugs and metabolites from urine and other biological matrices. Certify II is a mixed-mode cartridge packed with non-polar C8 and strong anion exchange (SAX) sorbent. It has been optimised for acidic drugs such as 11-nor-delta-9-tetrahydrocannibinol-carboxylic acid, salicylic acid, ibuprofen, acetaminophen and other compounds that possess both non-polar and anionic characteristics.

Supplier: Merck

Simazine CRM may also be used as given below: Development and validation of an ultrasonic-assisted dispersive liquid-liquid microextraction (UA-DLLME) method for sample extraction followed by gas chromatography-mass spectrometry based determination of endocrine-disrupting herbicides in the river and seawater samples. Determination of triazine pesticide residues in samples of apples pears carrots potatoes tomatoes avocado cucumber spinach bananas and oranges by modified QuEChERS and solid-phase extraction (SPE) procedures followed by liquid chromatography-photodiode array (LC-DAD) analysis. Multi-residue analysis of 67 pesticides in olive oil olives and avocado samples by liquid chromatography-tandem mass spectrometry (LC-MS/MS) to evaluate various clean-up sorbents. Quantitation of 20 pesticides in eel and shrimp samples by a scheduled multiple reaction monitoring (sMRM) method and QuEChERS with EDTA for sample extraction and purification. Analysis of 35 micropollutants including pesticides in water samples by liquid chromatography-tandem mass spectrometry (LC-MS/MS) after their solid-phase extraction. Simultaneous quantification of 58 pharmaceuticals and personal care products (PPCPs) and pesticides in water samples by solvent-based de-emulsification dispersive liquid-liquid microextraction (SD-DLLME) combined with liquid chromatography-tandem mass spectrometry (LCMS/MS).

Supplier: VARIAN

The water-wettable, hydroxylated exterior allows excellent flow, even with biological fluids. A gradient of polarity on the polymer surface shunts small analytes to the more hydrophobic centre of the polymer bead, where they are retained prior to the washing and elution steps. Plexa provides these performance enhancements due to a unique polymeric architecture with a non-retentive, hydroxylated, amide-free surface and a non-polar PS/DVB core for retaining small molecules.