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1747 results for "Analytical Standards"

1747 Results for: "Analytical Standards"

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Initial Calibration Verification Standard 1A, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

Initial Calibration Verification for CLP Methods
The US EPA retains analytical services through the Contract Laboratory Program (CLP). The CLP follows detailed SOPs derived from EPA methods. The CLP methods require calibration of analytical instrumentation whithin the expected quantitative range (ICAL standards) and additional CLP QA standards (ICV standards) to verify the calibration curve at each of the selected wavelengths that wil be used for sample analysis.

Our verification standards contain all of the elements on the TAL list and are independent standards for testing an instruments calibration curve. SPEX CertiPrep's ICV standards are designed to be used with their corresponding instrument calibration standards (ICAL).

We recommend dilution of ICV standards to a range within your instruments calibration curve. A dilution of 20-fold is recommended.

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Hypersil™ PREP BDS C18 HPLC Columns

Supplier: Thermo Scientific

Easily scale up your analytical method using Thermo Scientific™ Hypersil™ PREP BDS C18 reversed phase preparative HPLC columns.

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L-Isoleucine, Reference Standard

L-Isoleucine, Reference Standard

Supplier: USP

USP Reference Standards are specified for use in conducting official USP–NF tests and assays. USP also provides Reference Standards specified in the Food Chemicals Codex as well as authentic substances—high-quality chemical samples—as a service to analytical, clinical, pharmaceutical and research laboratories. To confirm accuracy and reproducibility, USP Reference Standards are rigorously tested and evaluated by multiple independent laboratories including USP, commercial, regulatory, and academic labs. USP also provide publicly available, official documentary standards for pharmaceutical ingredients in the USP–NF that link directly with our primary reference standards.

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PLAQPRO® Lp-PLA2 Assay, Enzo Life Sciences

Supplier: Enzo Life Sciences

Enzyme activity kit to measure Lp-PLA2 activity in  serum samples

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Gentamicin Sulfate, Reference Standard

Gentamicin Sulfate, Reference Standard

Supplier: USP

USP Reference Standards are specified for use in conducting official USP–NF tests and assays. USP also provides Reference Standards specified in the Food Chemicals Codex as well as authentic substances—high-quality chemical samples—as a service to analytical, clinical, pharmaceutical and research laboratories. To confirm accuracy and reproducibility, USP Reference Standards are rigorously tested and evaluated by multiple independent laboratories including USP, commercial, regulatory, and academic labs. USP also provide publicly available, official documentary standards for pharmaceutical ingredients in the USP–NF that link directly with our primary reference standards.

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Potassium hydrogen phthalate ≥99.95%, crystals ACS, Reagent Special for acid-base titration

Supplier: Spectrum Chemical Mfg. Corp.

Potassium Hydrogen Phthalate, Acidimetric Standard, Crystal, Reagent Special, ACS is used in analytical chemistry as a disintegrating agent can be used as a buffering agent (in combination with hydrochloric acid (HCl) or sodium hydroxide (NaOH). As an ACS grade Reagent, Spectrum Chemical manufactured Potassium Hydrogen Sulfate is used as the quality standard against which other Potassium Hydrogen Sulfate substances are graded. it has met the toughest regulatory standards for quality and pureness

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ICP Contract Required Detection Limit Standard 2 and 2A, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 & ILM 05.3 Standards for ICP
For ILM 05.3, a standard must be run at the Contract Required Detection Limits (CRDL). To verify linearity near the CRQL, this standard is analyzed at the beginning of the analysis run, after the ICV/ICB and before the ICSA and ICSAB. In addition, this standard must be run at a frequency of not less than 20 analytical samples and at the end of the analysis run, followed by the ICSA/ISCAB. The sequence order is CCV, CCB, CRI, ICSA, ICSAB, CCV, and CCB. For ISM 01.2, at least one of your calibration standards must be at the Contract Required Detection Limit (CRDL). This standard, when diluted, can be used as a calibration standard to fulfill this requirement.

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ICP Spike Sample 4, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
Our spike standard, SPIKE-4, provides all of the analytes required for the IC, ICP-AES and the AA spike.

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ICP Alternate Interferents A, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

Alternate Standards
We also provide a solution of alternate interferents and alternate analysis. Alternate interferents A (INT-A2) and alternate analytes B (INT-B2) may be prepared in combination with the INT-A1 and INT-B3 solutions mentioned, or any combination involving the four solutions, depending on the analytes and interferents of interest to you. We provides ICP-MS interferents and interferent check solutions for SW-845.

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ICP Spike Sample 1, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ILM 02.0 Standards for ICP
Our spike standard, SPIKE-1, provides all of the analytes required for the ICP-AES and the AA spike. Add 1 ml of SPIKE-1 to aqueous samples and 2 ml of SPIKE-1 to solid samples prior to digestion.

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ICP-MS Interferents Check Solution A3 (for SOW-846), SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

Alternate Standards
We also provide a solution of alternate interferents and alternate analysis. Alternate interferents A (INT-A2) and alternate analytes B (INT-B2) may be prepared in combination with the INT-A1 and INT-B3 solutions mentioned, or any combination involving the four solutions, depending on the analytes and interferents of interest to you. We provides ICP-MS interferents and interferent check solutions for SW-845.

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ICP-MS Contract Required Detection Limit Standard 2, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 Standards for ICP-MS
For ISM 01.2, at least one of your calibration standards must be at the Contract Required Detection Limit (CRDL). This standard, when diluted, can be used as a calibration standard to fulfill this requirement.

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OPTI-GUARD® Guard Columns, 1 mm

OPTI-GUARD® Guard Columns, 1 mm

Supplier: Optimize

OPTI-GUARD® sets the standard for extremely low impact, easy to use pre-column protection. Designed for use with analytical (Int.Ø: 4.6, 3.0 mm) and narrow-bore (Int.Ø: 2.1, 1.0 mm) columns, the patented floating stem design automatically adjusts to any manufacturer's tube stop depth for a zero-dead-volume connection every time.

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8330 Calibration Mix #1 (7 components), Restek

8330 Calibration Mix #1 (7 components), Restek

Supplier: Restek

EPA method 8330 is used to measure explosives residues in water and soil samples, using HPLC with UV detection. Target analytes are nitroaromatic and nitramine explosives and their degradation products. Obtaining pure, neat compounds for Method 8330 reference standards can be very difficult. To ensure the highest quality standards, Restek's Quality Control (QC) lab confirms the identity and purity of mixture components and solvents using one or more of the following techniques: GC-FID, HPLC, GC-ECD, GC-MS, LC-MS, refractive index, and melting point.

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8330 Calibration Mix #2 (7 components), Restek

8330 Calibration Mix #2 (7 components), Restek

Supplier: Restek

EPA method 8330 is used to measure explosives residues in water and soil samples, using HPLC with UV detection. Target analytes are nitroaromatic and nitramine explosives and their degradation products. Obtaining pure, neat compounds for Method 8330 reference standards can be very difficult. To ensure the highest quality standards, Restek's Quality Control (QC) lab confirms the identity and purity of mixture components and solvents using one or more of the following techniques: GC-FID, HPLC, GC-ECD, GC-MS, LC-MS, refractive index, and melting point.

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ICP Analytes B3, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B3). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B3 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B3 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

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Dipotassium disulfate, fused, powder ACS

Supplier: Spectrum Chemical Mfg. Corp.

Potassium Hydrogen Sulfate, Fused, Powder, Reagent, ACS is actually a fused mixture potassium hydrogen sulfate and potassium pyrosulfate otherwise known as the dipotassium salt of disulfuric acid. It's used in analytical chemistry as a disintegrating agent. As an ACS grade quality reagent, its chemical specifications are the de facto standards for chemicals used in many high-purity applications and typically designate the highest quality chemical available for laboratory use. Spectrum Chemical manufactured Reagent ACS grade products meet the toughest regulatory standards for quality and purity

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ICP-MS Interferents B3 with Mercury, 2 µg/ml (2 ppm), SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

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ICP-MS Interferents B3 without Mercury, 2 µg/ml (2 ppm), SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

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ICP-MS Analytes B4, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

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ICP Interferents A1, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.

The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.

US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:

• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements

CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B3). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B3 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B3 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

CLP ILM 02.0 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B1). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B1 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B1 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.

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Acclaim™ Trinity P2 Pharmaceutical Counterion Analysis Columns, Thermo Scientific

Acclaim™ Trinity P2 Pharmaceutical Counterion Analysis Columns, Thermo Scientific

Supplier: Thermo Scientific

The Thermo Scientific™ Acclaim™ Trinity™ P2 column is a high-performance, silica-based column specifically designed for separation of pharmaceutical mono- and multi-valent counterions by high-performance liquid chromatography (HPLC). This column was engineered for analytical chemists who need simple, robust, fast, generic methods. The Acclaim Trinity P2 columns provide an effective solution for counterion analysis using one column and one method on a standard HPLC instrument.

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N-Methyl-2-pyrrolidone (NMP) ≥99% ACS

Supplier: Spectrum Chemical Mfg. Corp.

1-Methyl-2-pyrrolidone, Reagent, ACS is a laboratory analytical reagent that is miscible with water and several other solvents, including ethyl acetate, chloroform, benzene and alcohols and ketones. 1-METHYL-2-PYRROLIDINONE, REAGENT, ACS is colorless to slightly yellow, and is used in the processing of petrochemicals to recover pure hydrocarbons. It is also commonly used to dissolve a broad range of chemicals, in particular polymers. There are several industrial uses, including treating surfaces of textiles, resins and plastics, as well as for stripping paint. As an ACS grade Reagent, Spectrum Chemical manufactured 1-Methyl-2-pyrrolidinone is used as the quality standard against which other substances are graded and has met the toughest regulatory standards for quality and pureness

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Performance Check Solution for US EPA Method 508, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

Pesticides, PCBs and Herbicides

The EPA is tasked with the monitoring of environmental systems as they pertain to contamination and human health. The methods issued by the EPA are created to respond to specific toxins or persistent organic pollutants (POPs) found in environmental samples such as soil, source water, drinking water, and waste. In particular, pollutants such as polychlorinated biphenyls (PCBs), which were in widespread industrial use up until their restriction, are of concern due to their stable and persistent nature in the environment. Another group of chemicals of high concern is the hundreds of commercial pesticides and herbicides in use in the world today. Pesticides, from algaecides to virucides, are used in large quantities in industrial and private agriculture. The concern over human pesticide exposure over the past few decades has led to extensive monitoring of these pesticides. It has been reported that over 98% of insecticides and 95% of herbicides affect areas other than their intended target product. It is essential that monitoring agencies have accurate standard mixes to measure the pesticide levels in the environment.

Many new pesticides are now being tested using highly sensitive LC/MS techniques, in addition to traditional GC techniques, to determine minute amounts of residue in environmental samples and food products.

At SPEX CertiPrep, we facilitate ease of monitoring and testing of pesticides by creating pesticide test mixes to suit your monitoring needs. SPEX CertiPrep is the leader in offering pesticide standards designed to work within EPA, AOAC and FDA analytical testing methods using all of the leading analytical techniques: LC, LC/MS, GC, and GC/MS. Many pesticide standard mixes are readily available in our catalog along with a large list of single pesticide standards. In addition, custom pesticide mixes can be made to your specifications to create a mix that meets your needs.

US EPA Method 508 is an analytical method for the monitoring of organochlorine pesticides and PCBs in drinking water and ground water by GC/ECD

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Method 531 Analyte Mix A, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

Pesticides, PCBs and Herbicides

The EPA is tasked with the monitoring of environmental systems as they pertain to contamination and human health. The methods issued by the EPA are created to respond to specific toxins or persistent organic pollutants (POPs) found in environmental samples such as soil, source water, drinking water, and waste. In particular, pollutants such as polychlorinated biphenyls (PCBs), which were in widespread industrial use up until their restriction, are of concern due to their stable and persistent nature in the environment. Another group of chemicals of high concern is the hundreds of commercial pesticides and herbicides in use in the world today. Pesticides, from algaecides to virucides, are used in large quantities in industrial and private agriculture. The concern over human pesticide exposure over the past few decades has led to extensive monitoring of these pesticides. It has been reported that over 98% of insecticides and 95% of herbicides affect areas other than their intended target product. It is essential that monitoring agencies have accurate standard mixes to measure the pesticide levels in the environment.

Many new pesticides are now being tested using highly sensitive LC/MS techniques, in addition to traditional GC techniques, to determine minute amounts of residue in environmental samples and food products.

At SPEX CertiPrep, we facilitate ease of monitoring and testing of pesticides by creating pesticide test mixes to suit your monitoring needs. SPEX CertiPrep is the leader in offering pesticide standards designed to work within EPA, AOAC and FDA analytical testing methods using all of the leading analytical techniques: LC, LC/MS, GC, and GC/MS. Many pesticide standard mixes are readily available in our catalog along with a large list of single pesticide standards. In addition, custom pesticide mixes can be made to your specifications to create a mix that meets your needs.

US EPA Method 531 is an analytical method for the monitoring of n-methylcarbamoyloximes and n-methylcarbamates in drinking water and ground water by HPLC and a fluorescence detector

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Initial Combination Calibration Standard for US EPA Method 8082 and CLP Series Methods, SPEX CertiPrep

Supplier: SPEX CERTIPREP LLC

Pesticides, PCBs and Herbicides

The EPA is tasked with the monitoring of environmental systems as they pertain to contamination and human health. The methods issued by the EPA are created to respond to specific toxins or persistent organic pollutants (POPs) found in environmental samples such as soil, source water, drinking water, and waste. In particular, pollutants such as polychlorinated biphenyls (PCBs), which were in widespread industrial use up until their restriction, are of concern due to their stable and persistent nature in the environment. Another group of chemicals of high concern is the hundreds of commercial pesticides and herbicides in use in the world today. Pesticides, from algaecides to virucides, are used in large quantities in industrial and private agriculture. The concern over human pesticide exposure over the past few decades has led to extensive monitoring of these pesticides. It has been reported that over 98% of insecticides and 95% of herbicides affect areas other than their intended target product. It is essential that monitoring agencies have accurate standard mixes to measure the pesticide levels in the environment.

Many new pesticides are now being tested using highly sensitive LC/MS techniques, in addition to traditional GC techniques, to determine minute amounts of residue in environmental samples and food products.

At SPEX CertiPrep, we facilitate ease of monitoring and testing of pesticides by creating pesticide test mixes to suit your monitoring needs. SPEX CertiPrep is the leader in offering pesticide standards designed to work within EPA, AOAC and FDA analytical testing methods using all of the leading analytical techniques: LC, LC/MS, GC, and GC/MS. Many pesticide standard mixes are readily available in our catalog along with a large list of single pesticide standards. In addition, custom pesticide mixes can be made to your specifications to create a mix that meets your needs.

US EPA Method 8082 is an analytical method for the monitoring of PCBs in environmental samples by GC/ECD or GC/ELCD

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Copper(II) sulfate, anhydrous ≥98%, powder, Reagent Grade

Supplier: Spectrum Chemical Mfg. Corp.

Cupric Sulfate, Anhydrous, Powder, Reagent also known as Copper(II) Sulfate is an inorganic pale green or gray-white powder. As an analytical reagent it is used in Benedict's solution and Fehling's solution to test for reducing sugars and in Biuret reagent to test for proteins. The Reagent grade denotes that this chemical is the highest quality commercially available and that the American Chemical Society has not officially set any specifications for this material. Spectrum Chemical manufactured Reagent grade products meet the toughest regulatory standards for quality and purity.

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Poly(vinylidene fluoride)

Supplier: Thermo Scientific Chemicals

Poly(vinylidene fluoride) is useful in coatings, film, filter cloth, instrument linings, filtration membranes, pump parts, linings and valves. It is also employed as a material for transducers in devices such as headphones, microphones and sonic detectors. It is also essential for piezoelectric and electrostrictive applications. In addition, it is useful for monofilament fishing lines replacing nylon monofilament. It acts as a standard binder used in the production of composite electrodes for lithium ion batteries. It serves as a high grade insulator for wires, nanomaterials and pressure sensors. It is utilized to make filters which are used to prepare samples for high performance liquid chromatography and other advanced analytical techniques.
Notes: Incompatible with strong oxidizing agents.

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GsBP®-InoWax Polar, PEG GC Columns, GS-Tek

GsBP®-InoWax Polar, PEG GC Columns, GS-Tek

Supplier: General Separation Technologies, Inc.

Typical application: Alcohols II and III, Amines (low MW), Amines/ Alcohols/ Chlorides, Aromatics analysis: ASTM D16 analytes, Aromatics II, Blood alcohol, Bourbon, Branched alcohols, BTEX, Chlorinated Isooctane, Citronella java oil, Esters III, Ethylene oxide, FAME Standard I, FAMEs (Coca Butter), Fast styrene analysis, Flavor volatiles, Formaldehyde Underivatized, Fragrance allergens, Fragrance Reference Standard II, Free Fatty Acids, Free Organic Acids/C4-C5 Isomers, Impurities in Ethylbenzene, Impurities in mixed xylenes, Impurities in p-Xylene-ASTM D3798, Impurities in styrene, Industrial Solvent, Lavender Oil Spiked with Camphor, Monomers in latex paint by headspace, Mushroom aroma (Synthetic), Nitrosamines, Nutmeg oil, Organic acids, Phenols III, Polyunsaturated fatty acid methyl esters, Rapeseed oil, Rapid analysis of water in organic solvents, Solvents I, II, Spearmint oil, Strawberry syrup, Sulphur and Selenium in Garlic by Headspace, Tramanian lavander oil, Volatile organics, Volatile sulfurs.

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Ion Chromatography (IC) Anion and Cation Check Standards, VWR Chemicals BDH®

Ion Chromatography (IC) Anion and Cation Check Standards, VWR Chemicals BDH®

Supplier: VWR International

Ion chromatography (IC) is an analytical process for the separation of ions based on charge affinity. IC can be used for a variety of different kinds of charged analytes from single elements to large proteins.

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