You searched for: Cationic Standards
Avantor offers a wide range of certified cationic standards designed for instrument calibration in ion-exchange chromatography (IC) applications, which can be applied toward environmental or food analysis and quality control. IC is an analytical technique used for the separation and quantification of anions and cations in aqueous samples. Avantor offers high-purity, well-defined reference materials ideal for low-ppm level quantification or trace analysis. Bottles of cationic standards are available for a range of elements.
Aluminum, AAS standard solution, Specpure®, Al 1000 µg/ml, Thermo Scientific
Supplier: Thermo Scientific Chemicals
Molecular Formula: Al in 5% HCl
Physical Form: Liquid
UN No.: 1789
MDL No.: MFCD00134029
Expand 2 Items
ICP-MS Contract Required Detection Limit Standard, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
Expand 2 Items
Barium, plasma standard solution, Specpure®, Ba 1000µg/ml, Thermo Scientific
Supplier: Thermo Scientific Chemicals
Molecular Formula: Ba(NO3)2 in 5% HNO3
Physical Form: Liquid
UN No.: 3264
MDL No.: MFCD00134031
Expand 3 Items
Interference Check Standard AB(ICS-AB) Solution, Specpure®, Thermo Scientific
Supplier: Thermo Scientific Chemicals
Molecular Formula: Matrix: 5% HNO3/tr. tartaric acid
Physical Form: Liquid
UN No.: 3264
MDL No.: MFCD00147272
Expand 1 Items
Precious Metals, plasma standard solution, Specpure®, Au, Ir, Os, Pd, Pt, Re, Rh, Ru @ 100µg/ml, Thermo Scientific
Supplier: Thermo Scientific Chemicals
Molecular Formula: Matrix: 20% HCl
Physical Form: Liquid
UN No.: 1789
MDL No.: MFCD00151264
Expand 2 Items
Claritas PPT® Grade Heavy Metals Testing Kit, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
Heavy Metals & Minerals Testing Kits
For routinely analyzed Heavy Metals and Minerals
Heavy Metals and Minerals Testing Kits are designed for routinely analyzed heavy metals and minerals. All kits come with six, 30 ml standards which includes a nitiric acid blank for easy dilution. Conveniently packaged in a sturdy, heavy-duty carton, these kits are perfect to store on a lab bench or in a cabinet. The 30 ml standards ship non-hazardous, saving money on shipping costs. The smaller volume also allows for less hazardous waste should the standard expire before its contents are used.
Expand 1 Items
ICP Spike Sample 4, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
Our spike standard, SPIKE-4, provides all of the analytes required for the IC, ICP-AES and the AA spike.
Expand 1 Items
ICP Spike Sample 1, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ILM 02.0 Standards for ICP
Our spike standard, SPIKE-1, provides all of the analytes required for the ICP-AES and the AA spike. Add 1 ml of SPIKE-1 to aqueous samples and 2 ml of SPIKE-1 to solid samples prior to digestion.
Expand 2 Items
ICP-MS Contract Required Detection Limit Standard 2, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 Standards for ICP-MS
For ISM 01.2, at least one of your calibration standards must be at the Contract Required Detection Limit (CRDL). This standard, when diluted, can be used as a calibration standard to fulfill this requirement.
Expand 1 Items
ICP Alternate Interferents A, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
Alternate Standards
We also provide a solution of alternate interferents and alternate analysis. Alternate interferents A (INT-A2) and alternate analytes B (INT-B2) may be prepared in combination with the INT-A1 and INT-B3 solutions mentioned, or any combination involving the four solutions, depending on the analytes and interferents of interest to you. We provides ICP-MS interferents and interferent check solutions for SW-845.
Expand 1 Items
ICP-MS Interferents Check Solution A3 (for SOW-846), SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
Alternate Standards
We also provide a solution of alternate interferents and alternate analysis. Alternate interferents A (INT-A2) and alternate analytes B (INT-B2) may be prepared in combination with the INT-A1 and INT-B3 solutions mentioned, or any combination involving the four solutions, depending on the analytes and interferents of interest to you. We provides ICP-MS interferents and interferent check solutions for SW-845.
Expand 1 Items
ICP-MS Spike Sample 4, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 Standards for ICP-MS
Our spike standard, CL-SPIKE-4, provides all of the analytes required for the ICP-MS and the AA spike. Add 1 ml of CL-SPIKE-4 to aqueous samples and 2 ml of CL-SPIKE-4 to solid samples prior to digestion.
CLP ILM 05.3 Standards for ICP-MS
Our spike standard, CL-SPIKE-4, provides all of the analytes required for the ICP-MS.
Expand 1 Items
Initial Calibration Verification Standard 3, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
Initial Calibration Verification for CLP Methods
The US EPA retains analytical services through the Contract Laboratory Program (CLP). The CLP follows detailed SOPs derived from EPA methods. The CLP methods require calibration of analytical instrumentation whithin the expected quantitative range (ICAL standards) and additional CLP QA standards (ICV standards) to verify the calibration curve at each of the selected wavelengths that wil be used for sample analysis.
Our verification standards contain all of the elements on the TAL list and are independent standards for testing an instruments calibration curve. SPEX CertiPrep's ICV standards are designed to be used with their corresponding instrument calibration standards (ICAL).
We recommend dilution of ICV standards to a range within your instruments calibration curve. A dilution of 20-fold is recommended.
Expand 1 Items
ICP Contract Required Detection Limit Standard 2 and 2A, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 & ILM 05.3 Standards for ICP
For ILM 05.3, a standard must be run at the Contract Required Detection Limits (CRDL). To verify linearity near the CRQL, this standard is analyzed at the beginning of the analysis run, after the ICV/ICB and before the ICSA and ICSAB. In addition, this standard must be run at a frequency of not less than 20 analytical samples and at the end of the analysis run, followed by the ICSA/ISCAB. The sequence order is CCV, CCB, CRI, ICSA, ICSAB, CCV, and CCB. For ISM 01.2, at least one of your calibration standards must be at the Contract Required Detection Limit (CRDL). This standard, when diluted, can be used as a calibration standard to fulfill this requirement.
Expand 2 Items
ICP Analytes B3, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B3). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B3 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B3 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
Expand 1 Items
Initial Calibration Verification Standard 1A, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
Initial Calibration Verification for CLP Methods
The US EPA retains analytical services through the Contract Laboratory Program (CLP). The CLP follows detailed SOPs derived from EPA methods. The CLP methods require calibration of analytical instrumentation whithin the expected quantitative range (ICAL standards) and additional CLP QA standards (ICV standards) to verify the calibration curve at each of the selected wavelengths that wil be used for sample analysis.
Our verification standards contain all of the elements on the TAL list and are independent standards for testing an instruments calibration curve. SPEX CertiPrep's ICV standards are designed to be used with their corresponding instrument calibration standards (ICAL).
We recommend dilution of ICV standards to a range within your instruments calibration curve. A dilution of 20-fold is recommended.
Expand 1 Items
ICP-MS Interferents B3 without Mercury, 2 µg/ml (2 ppm), SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
Expand 1 Items
ICP-MS Analytes B4, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
Expand 1 Items
ICP-MS Interferents B3 with Mercury, 2 µg/ml (2 ppm), SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 ml of CL-INT-A2 and 1 ml of CL-INT-B3 or CL-INT-B4 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
Expand 1 Items
Lead Standard Solutions, NIST
Supplier: Hach
Standard solutions for accuracy checks in lead determinations.
Expand 1 Items
ICP Interferents A1, SPEX CertiPrep
Supplier: SPEX CERTIPREP LLC
CLP Standards for ICP & ICP-MS
Our Contract Laboratory Program (CLP) standards allow you to Calibrate with Confidence®. The standards are to be used in conjunction with the Statement of Work for Inorganic Analysis; Multi-Media/Multi-Concentration Document Number ILM 05.3/ISM 01.2.
The final ICP check, performed in our own laboratories, is your stamp of assurance. We calibrate our instruments with traceable reference materials and show you the actual found value of the solution you receive, not just an ideal, calculated number as so many other standards manufacturers do. The combination of elements, concentrations and matrices listed have been diagnosed by SPEX CertiPrep for convenience of use and stability.
US EPA SOW ILM 05.3/ISM 01.2 gives specific procedures for the methods of analysis, target elements, and concentrationlevels. Standards are specified not only by the elements present and their relative concentrations, but also the order and frequency of running standards, blanks and samples. Details of these specifications may be found in the US EPA SOW ILM 05.3/ISM 01.2 in the following sections:
• Exhibit C, Inorganic Target Analyte List (TAL)
• Exhibit D, Analytical Methods
• Exhibit E, QA/QC Requirements
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B3). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B3 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B3 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.
CLP ILM 02.0 Standards for ICP
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (INT-A1) and Solution AB, a combination of interferents (INT-A1) and analytes (INT-B1). Solution A is prepared by diluting INT-A1 20-fold. Solution AB is prepared by diluting INT-A1 20-fold and INT-B1 100-fold; for example, 5 ml of INT-A1 and 1 ml of INT-B1 into a 100 ml volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.