"Solid Phase Extraction"
Solid phase extraction cartridges, Bond Elut™ C2
Supplier: VARIAN
Bond Elut™ C2 is a fairly non-polar sorbent because of the short chain length of the functional group. C2 is often used during the process of method development if analytes are retained too strongly on a C8 or C18 phase. The polarity of C2 is slightly lower than a cyano phase for polar interactions.
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Solid phase extraction cartridges, Bond Elut™ C18 EWP
Supplier: VARIAN
Bond Elut™ EWP is based upon standard particle size silica but with 500 Å pores to allow more efficient extraction of large molecules (>15000 MW), which are typically excluded from standard porosity silica phases.
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Solid phase extraction cartridges, Bond Elut™ Florisil
Supplier: VARIAN
Florisil is a magnesia-loaded silica gel, extremely polar in nature and ideal for the isolation of polar compounds from non-polar matrices.
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Solid phase extraction cartridges for pesticide residue cleanup
Supplier: Restek
Pesticide residue cleanup SPE cartridges are convenient with multiple adsorbent beds in a single cartridge. It is used in multiresidue pesticide analysis to remove matrix interferences and also exhibits good cleanup of dietary supplement extracts.
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Solid phase extraction cartridges, Bond Elut™ PH
Supplier: VARIAN
Bond Elut™ PH is a non-polar bonded silica material which exhibits a different selectivity to alkyl or aliphatic functionalised phases such as C8 or cyclohexyl. The electron density present in the aromatic ring affords an enhancement in the retention of conjugated or aromatic ring-containing analytes due to desirable pi-pi interactions.
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ASPEC® 274 system
Supplier: GILSON LCMS
This ASPEC® system for positive pressure solid phase extraction (SPE) automation maximises throughput by processing up to four samples in parallel. With its small footprint and multiple probes, it is the ideal choice for reproducible and efficient sample cleanup for clinical, forensic, doping, food, and environmental testing labs.
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Solid phase extraction cartridges, Bond Elut™ LMS
Supplier: VARIAN
Bond Elut™ LMS polymeric sorbent lets you elute without having to add amine modifiers, buffers, or acids. The elimination of secondary interactions means that elution of analytes can be achieved with pure organic solvents or HPLC mobile phase-compatible solvent mixtures of low ionic strength. These characteristics are crucial to allow compatibility with LC/MS or other delicate analytical techniques.
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Solid phase extraction cartridges, Bond Elut™ C1
Supplier: VARIAN
Due to the methyl group and subsequent low carbon load, Bond Elut™ C1 is the least retentive of all alkyl group bonded phases for non-polar compounds. However, due to the extensive end capping of this sorbent to mask polar silanol activity, retention and elution of polar and multi-functional analytes can still be achieved. Typical applications include plasma, urine and aqueous samples.
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Solid phase extraction cartridges, Bond Elut™ C18 OH
Supplier: VARIAN
Bond Elut™ C18 OH is a non-end capped version of the octadecyl bonded phases that enables the silanols on the silica surface to be more active. This low-load C18 has well-controlled silanol activity that permits the fractionation of metabolites and enhances retention of basic compounds compared to an endcapped C18. The pore size makes it a good choice for peptide extraction.
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Solid phase extraction cartridges, Bond Elut™ PPL
Supplier: VARIAN
Bond Elut™ PPL is a styrene-divinylvenzene (SDVB) polymer that has been modified with a proprietary non-polar surface. PPL will retain even the most polar classes of analytes, including phenols. The large particle size allows ease of flow for viscous or particulate rich water samples, while the high surface area and strong hydrophobicity ensure reproducible extractions with high recoveries upon elution. Bond Elut™ PPL is suitable for EPA Method 528 ‘Determination of Phenols in Drinking Water by SPE and Capillary GC/MS’.
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Solid phase extraction cartridge, Sep-Pak® XPoSure™ Plus
Supplier: WATERS
Specially designed for monitoring aldehydes in indoor air.
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Solid phase extraction cartridges, Bond Elut™ CBA
Supplier: VARIAN
CBA is a mid-polarity sorbent and weak cation exchanger (pKa 4,8). It can be used with a wider range of counter-ions than lower pKa sorbents like SCX and will demonstrate easier elution of quaternary amine functionalised analytes.
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Supelco® TraceCERT® Organic Reference Standard, Tebutam
Supplier: Merck
Tebutam CRM may also be used as given below:
Optimisation of sample extraction based on QuEChERS and dispersive-solid-phase extraction (d-SPE) clean-up for the multi-residue analysis of 120 pesticides 16 polycyclic aromatic hydrocarbons and 22 polychlorinated biphenyls by liquid and gas chromatography coupled with tandem mass spectrometry (MS/MS)
Evaluation of 250 pesticide residues extracted by QuEChERS method from 103 processed fruit samples using ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS)
Determination of 90 pesticides 16 polycyclic aromatic hydrocarbons and 22 polychlorinated biphenyls in honey samples by using QuEChERS combined with dispersive solid-phase extraction (SPME) for sample pre-treatment and liquid chromatography-triple-quadrupole tandem mass spectrometry and gas chromatography-ion-trap tandem mass spectrometry for quantitation
Screening and quantification of 569 pesticides in honeysuckle samples by a combination of ultrahigh-performance liquid chromatography (UHPLC) and quadrupole-Orbitrap high-resolution mass spectrometry
Simultaneous determination of 134 pesticide residues in tea samples using d-SPE extraction with a multi-functional filter (MFF) followed by ultra-high performance liquid chromatography (UPLC) and quadrupole time-of-flight mass spectrometry (TOF-MS).
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Solid phase extraction cartridges, Bond Elut™ CH
Supplier: Agilent
Bond Elut™ CH is a mid-polarity sorbent that exhibits unique selectivities for certain analytes. When employed as a non-polar sorbent, CH has the approximate polarity of a C₂ sorbent. Bond Elut™ CH is often a good choice when non-polar sorbents such as C₁₈, C₈ or C₂ do not provide the desired selectivity.
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Solid phase microextraction fibers
Supplier: VARIAN
Solid phase microextraction (SPME) is a technique for extracting analytes from solid, liquid or gaseous samples by adsorbing them onto the SPME fiber and then desorbing them into an inlet, either on a gas chromatograph (GC) or an HPLC system. SPME is amenable to automation using an autosampler or it can be performed manually as well.
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Solid phase extraction cartridges, Bond Elut™ Diol
Supplier: VARIAN
Bond Elut™ Diol (2OH) resembles unbonded silica in its tendency for strong hydrogen bonding with analytes. 2OH can also be employed in the non-polar mode because the hydrocarbon spacer on its functional group provides enough non-polar character for retention of hydrophobic analytes. Bond Elut™ Diol is a listed SPE device for the DIN 14333-1 method on benzimidazole fungicides.
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